| 光谱学与光谱分析 |
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| Purification of Sulfolene and Its UV-Vis and FTIR Spectral Analysis |
| JIA Tai-xuan1,2,LIU Zi-li1,2*,FENG Shi-hong3 |
1. College of Chemistry & Chemical Engineering, Guangxi University, Nanning 530004, China
2. College of Chemistry & Chemical Engineering, Guangzhou University, Guangzhou 510006, China
3. College of Materials Science & Chemical Engineering，Liaoning University of Technology, Jinzhou 121004, China |
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Abstract Purification of raw sulfolene was investigated by adsorption method using activated carbon and exchange resin, and the sulfolene was detected by UV-Vis, FTIR and XRD. FTIR spectra of sulfolene and sulfolane were especially analyzed. The results showed that it was the best way to purify industrial grade sulfolene by activated carbon connected exchange resin. The sulfolane with high quality was synthesized by purified sulfolene through catalytic hydrogenation with catalyst. The conversion efficiency was more than 99.8%. It could provide experimental data for the technical reform of industry equipment.
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Received: 2007-09-28
Accepted: 2007-12-29
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Corresponding Authors:
LIU Zi-li
E-mail: jiataixuan@163.com
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[1] LIN Bi-zhou, PEI Xiao-ke, ZHANG Jin-fei(林碧洲, 裴小科, 张进飞). Chinese Journal of Inorganic Chemistry(无机化学学报), 2004, 20: 1023.
[2] ZHANG Jin-fei, LIN Bi-zhou(张进飞, 林碧洲). Chinese Journal of Catalysis(催化学报), 2006, 27(1): 29.
[3] MA Hong-mei, ZHU Zhi-liang, ZHANG Rong-hua(马红梅, 朱志良, 张荣华). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2007, 27(1): 165.
[4] CHI Jiu-chun(迟久春). Chemical Engineering of Oil and Gas(石油与天然气化工), 1986, 15(1): 48.
[5] LIU Ying-xin, LI Xin-xue, WEI Xiong-hui(刘迎新, 李新学, 魏雄辉). Chemistry Bulletin(化学通报), 2004, 67(12): 869.
[6] Ali Babaei, McQuillan A James. Journal of Electroanalytical Chemistry, 1999, 462: 266.
[7] Tunde Alapi, Andras Dombi. Journal of Photochemistry and Photobiology A, Chemistry, 2007, 188: 409.
[8] Hrvoje Kusic, Natalija Koprivanac. Journal of Hazardous Materials B, 2006, 136: 632.
[9] QIN Chuan-xiao(秦川校). Spectrum Resolution of Organic Compound(有机化合物的波谱解析). Shanghai: East China University of Science and Technology Press(上海：华东理工大学出版社), 2007.
[10] NI Zhuo, NI Ying(倪 卓, 倪 颖). Journal of Natural Science of Helongjiang University(黑龙江大学自然科学学报), 1991, 8(2): 90. |
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