光谱学与光谱分析 |
|
|
|
|
|
Determination of the Amount of 13 Metal Elements in the Rape Pollen from Different Regions by Flame Atomic Absorption Spectrophotometry |
CHANG Yan-hong1,2,XUE Guo-qing1*,SONG Hai1,DI Duo-long3 |
1. Department of Chemistry, Key Laboratory of Resources and Environment Chemistry of West China, Hexi University,Zhangye 734000, China 2. Life Sciences and Chemistry School, Tianshui Normal University, Tianshui 741001, China 3. Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000,China |
|
|
Abstract The objective of the present paper was to determine the amount of metal elements in the rape pollen from different regions by flame atomic absorption spectrophotometry (FAAS). FAAS method was established for the determination of K, Na, Ca, Mg, Fe, Co, Ni, Cu, Zn, Mn, Cd, Cr and Pb in the rape pollen. The samples were incinerated and then digested with HNO3-HClO4(V∶V=4∶1) at 90-95 ℃ and under normal pressure. In the meantime, the optimum parameters of FAAS and the effects of solution medium on the results were studied. The analytical results of K, Na, Ca, Mg, Fe, Cu, Zn and Mn rape pollen from different habitats respectively were 4 248.00, 75.77, 312.10, 856.61, 599.53, 8.78, 27.82, 22.54 μg·g-1 and 7 585.75, 242.56, 287.88, 699.43, 1 020.65, 10.25, 40.44, 30.97 μg·g-1,while Co, Ni, Cd, Cr and Pb were not checked out in the samples. The results showed that the recovery of standard addition was 95.22%-105.49%, and the RSD(n=9) was 0.30%-5.00%. The characteristic method is quick, simple and convenient, and the results are satisfactory.
|
Received: 2006-05-10
Accepted: 2006-08-20
|
|
Corresponding Authors:
XUE Guo-qing
E-mail: xuegq@hxu.edu.cn
|
|
Cite this article: |
CHANG Yan-hong,XUE Guo-qing,SONG Hai, et al. Determination of the Amount of 13 Metal Elements in the Rape Pollen from Different Regions by Flame Atomic Absorption Spectrophotometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(06): 1235-1238.
|
|
|
|
URL: |
https://www.gpxygpfx.com/EN/Y2007/V27/I06/1235 |
[1] XUE Guo-qing, LIU Qing, HAN Xiao-mei, et al(薛国庆,刘 青,韩晓梅,等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2006, 26(6): 1173. [2] XUE Guo-qing, LIU Qing, REN Xue-feng, et al(薛国庆,刘 青,任雪峰,等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2004, 24(11): 1461. [3] ZENG Zhi-jiang, YAN Wei-yu, WANG Kai-fa(曾志将,颜伟玉,王开发). Chinese Bulletin of Botany(植物学通报), 2002, 19(4): 488. [4] WANG Kai-fa(王开发). Nutritional Components of Pollen and Utilization of Natural Resources of Pollen(花粉营养成分与花粉资源利用). Shanghai: Fudan University Press(上海:复旦大学出版社),1993. 37.
|
[1] |
LIU Hong-wei1, FU Liang2*, CHEN Lin3. Analysis of Heavy Metal Elements in Palm Oil Using MP-AES Based on Extraction Induced by Emulsion Breaking[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3111-3116. |
[2] |
JIN Xu-guang1, 2, WANG Jin-zhuan1, 2*, LI Bei1, 2, QUE Wan-ting1, 2, WANG Liang1, 2, ZHANG Fan1, 2, ZHANG Chi1, ZHOU Jun-gui1, FU Rong-jin1. Quantification of Au in Gold Ornaments Obtained by Different Electroformed Process[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2755-2760. |
[3] |
WU Lei1, LI Ling-yun2, PENG Yong-zhen1*. Rapid Determination of Trace Elements in Water by Total Reflection
X-Ray Fluorescence Spectrometry Using Direct Sampling[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 990-996. |
[4] |
WU Bing, YANG Ke-ming*, GAO Wei, LI Yan-ru, HAN Qian-qian, ZHANG Jian-hong. EC-PB Rules for Spectral Discrimination of Copper and Lead Pollution Elements in Corn Leaves[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3256-3262. |
[5] |
ZHENG Pei-chao, LIU Ran-ning, WANG Jin-mei, FENG Chu-hui, HE Yu-tong, WU Mei-ni, HE Yu-xin. Solution Cathode Glow Discharge-Atomic Emission Spectroscopy Coupled With Hydride Generation for Detecting Trace Mercury and Tin in Water[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1139-1143. |
[6] |
MENG Ru2,4, DU Jin-hua1,2*, LIU Yun-hua1,2, LUO Lin-tao1,3, HE Ke1,2, LIU Min-wu1,2, LIU Bo1,3. Exploration of Digestion Method for Determination of Heavy Metal Elements in Soil by ICP-MS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(07): 2122-2128. |
[7] |
ZHANG Chao, ZHU Lin, GUO Jin-jia*, LI Nan, TIAN Ye, ZHENG Rong-er. Laser-Induced Breakdown Spectroscopy for Heavy Metal Analysis of Zn of Ocean Sediments[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(11): 3617-3622. |
[8] |
ZHENG Pei-chao1, HE Miao1, WANG Jin-mei1*, WANG Ning-shen1, LI Wei-qi1, LUO Yuan-jiang1, DONG Da-ming2, ZHENG Kun-peng1, YAN Bo-wen1. Ca and Mg Analysis in Solution by Solution Cathode Glow Discharge Combined with Standard Addition Method and Background Removal[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(01): 271-276. |
[9] |
YANG Chang-bao1, LIU Na2*, KUAI Kai-fu3. Research on Relationship between Spectral Characteristics, Physical Parameters and Metal Elements of Rocks in Xingcheng Area[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(09): 2953-2965. |
[10] |
YANG Lu-wei1, LI Ming2*, GAO Wen-feng2, LIU Gang1, WANG Yun-feng2, WANG Wei1, LI Kun1. Determination of Heavy Metal Elements in Stagnation Water of Flat-Plate Solar Collectors With ICP-OES[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(06): 1947-1952. |
[11] |
LIU Bing-bing, LIU Jia, ZHANG Chen-ling, HAN Mei, JIA Na, LIU Sheng-hua*. Preconcentration and Determination of Heavy Metals in Water Samples by Ion Exchange Resin Solid Phase Extraction with Inductively Coupled Plasma Atomic Emission Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(12): 3917-3922. |
[12] |
ZHANG Li-jiao1,2, LAI Wan-chang1, XIE Bo2, 3, HUANG Jin-chu1, LI Dan1, WANG Guang-xi1, YANG Qiang1, CHEN Xiao-li1. The Effect of Filterson on the Determination of Trace Heavy Metal Cd in Light Matrix by Energy Dispersive X-Ray Fluorescence Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(06): 1917-1921. |
[13] |
ZHENG Pei-chao, ZHAI Xiang, WANG Jin-mei*, YANG Rui. Analysis of Solution Cathode Glow Discharge Atomic Emission Spectroscopy by the Multiple Linear Regression Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(10): 3209-3213. |
[14] |
YANG Chang-bao1, LIU Na1*, ZHOU Zhen-chao1, LI Shang-nan1,2, ZHANG Chen-xi3, SONG Jiang-tao1. Research on the Relationship between Main Rock Metal Elements Content,Physical Parameters and Spectral Features in Tahe Area[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(08): 2569-2574. |
[15] |
SUN Qian-qian, DU Min, GUO Lian-bo, HAO Zhong-qi, YI Rong-xing, LI Jia-ming, LIU Jian-guo, SHEN Meng, LI Xiang-you*, ZENG Xiao-yan, LU Yong-feng. Fast Identification of Plastics with Laser-Induced Breakdown Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(07): 2205-2209. |
|
|
|
|