| 光谱学与光谱分析 |
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| Filter Coated with Phenyl Fluorone for Enrichment and Determination of Indium by GFAAS |
| LI Xing-yang,WEI Xiao-ling,GONG Qi* |
| College of Chemistry and Chemical Engineering, Guangxi University, Nanning 530014, China |
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Abstract The filter fiber column coated with phenyl fluorone was extended to pre-concentrate trace amount of indium determined by GFAAS. The optimized condition for filter fiber coated with phenyl fluorone was obtained. The enrichment condition was achieved when the pregnant solution at pH 5 flowed through the filter fiber column at the rate of less than 2.0 mL·min-1,then 8mL HNO3 of 5.00 mol·L-1 was used as an eluent. With a general graphite tube coated with tungsten and silver as matrix modifier, the sensitivity was enhanced with GFAAS. The method was validated by the determination of trace indium in water, artificial zinc, and aluminium samples. The detection limit of the method was 0.32 ng·mL-1,the recovery was in the range of 95.0%-101%, and the RSD was between 1.8% and 7.0％.
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Received: 2006-03-16
Accepted: 2006-07-26
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Corresponding Authors:
GONG Qi
E-mail: gongqi@gxu.edu.cn
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| Cite this article: |
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LI Xing-yang,WEI Xiao-ling,GONG Qi. Filter Coated with Phenyl Fluorone for Enrichment and Determination of Indium by GFAAS [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(06): 1225-1228.
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| URL: |
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https://www.gpxygpfx.com/EN/Y2007/V27/I06/1225 |
[1] ZHOU Qing-hai, ZHOU Xiao-hua(周清海, 周晓华). Journal of Instrumental Analysis(分析测试学报), 1997, 16(4): 35.
[2] LIU Wei, WU Xian-long, ZHU Ai-li(刘 伟, 吴宪龙, 朱爱丽). Analysis Laboratory(分析试验室), 1999, 18(2): 31.
[3] WEI Qin, DU Bin, WU Dan, et al(魏 琴, 杜 斌, 吴 丹, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2005, 25(5): 772.
[4] SAI Yin, LI Sheng, HAN Fu-bin(赛 音, 李 胜, 韩福彬). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2004, 24(11): 1404.
[5] WANG Yu-xing, ZHANG Jian-hua, HAO Jin-nü, et al(王玉兴, 张建华, 郝金女, 等). Chinese Journal of Analytical Chemistry(分析化学), 1994, 22(6): 623.
[6] Martúnez A N C, Adela Bermejo Barrera, Bermejo B P. Talanta, 2005, 66: 646.
[7] GONG Qi, LI Xiang-xin, WEI Xiao-ling, et al(龚 琦，李向欣，韦小玲，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2006，26(6)：1162. |
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