光谱学与光谱分析 |
|
|
|
|
|
Quantitative Determination of Glucose by Internal Standard Laser Raman Spectra |
WU Xiao-qiong1,ZHENG Jian-zhen1,LIU Wen-han1*,LIN Zhen-xing2 |
1. College of Chemical Engineering and Material Science,Zhejiang University of Technology,Hangzhou 310032,China 2. Ningbo Entry-Exit Inspection and Quarantine Bureau of the People’s Republic of China,Ningbo 315012,China |
|
|
Abstract In the present paper we report quantitative analysis of glucose using internal standard laser Raman spectra. A good linear correlation was observed between the intensities of the —COO band at 1 125 cm-1 using excition wavelength of 632.81 nm(r=0.998 8) and the glucose concentration over the range 0-1.8 mol·L-1. Band intensities were normalized against an internal standard (water band at 1 643 cm-1),and the limit of detection (L.O.D.) of glucose is 0.022 7 mol·L-1. The interference ions would not influence the quantitative analysis. When this method was used to determine 5% glucose NaCl,5% glucose,and 10% glucose injections,the result showed that the recoveries are 71.88%-126.31%,81.02%-124.89% and 74.87%-121.32%,and the RSDs are 5.44%,4.34% and 0.94%,respectively. The non destructive,non intrusive nature of the method makes internal standard laser Raman spectra a convenient,accurate,and green quantitative analysis method.
|
Received: 2006-03-27
Accepted: 2006-07-08
|
|
Corresponding Authors:
LIU Wen-han
E-mail: LiuWH@mail.hz.zj.cn
|
|
Cite this article: |
WU Xiao-qiong,ZHENG Jian-zhen,LIU Wen-han, et al. Quantitative Determination of Glucose by Internal Standard Laser Raman Spectra[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(07): 1344-1346.
|
|
|
|
URL: |
https://www.gpxygpfx.com/EN/Y2007/V27/I07/1344 |
[1] SHI Yu-zhen,CHEN Zhi-chun,LIN Xian-fu(施玉珍,陈志春,林贤福). Chinese Journal of Analytical Chemistry(分析化学),2005,33(2): 272. [2] WANG Rong,FENG Min,WU Wei-hong,et al(王 荣,冯 敏,吴卫红,等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2005,25(9): 1422. [3] CHEN Yong,ZHOU Yao-qi,ZHANG Da-gang(陈 勇,周瑶琪,章大港). Chinese Journal of Light Scattering(光散射学报),2003,15(4): 216. [4] WANG Bin,WANG Jing,YU Jiang,et al(王 斌,王 靖,余 江,等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),1999,19(5): 674. [5] Shadi I T. Spectrochimica Acta Part,A,2003,59: 2213. [6] GUO Ping,YUAN Ya-li,XIONG Ping(郭 萍,袁亚莉,熊 平). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2004,24(10): 1210. [7] LIU Wen-han,ZHANG Dan,WU Xiao-qiong,et al(刘文涵,张 丹,吴小琼,等). Journal of Zhejiang University of Technology(浙江工业大学学报),2005,33(6): 608. [8] LIU Wen-han,ZHANG Dan,ZHENG Jian-zhen,et al(刘文涵,张 丹,郑建珍,等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2006,26(5): 865. |
[1] |
LI Yu1, ZHANG Ke-can1, PENG Li-juan2*, ZHU Zheng-liang1, HE Liang1*. Simultaneous Detection of Glucose and Xylose in Tobacco by Using Partial Least Squares Assisted UV-Vis Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 103-110. |
[2] |
LIU Hao-dong1, 2, JIANG Xi-quan1, 2, NIU Hao1, 2, LIU Yu-bo1, LI Hui2, LIU Yuan2, Wei Zhang2, LI Lu-yan1, CHEN Ting1,ZHAO Yan-jie1*,NI Jia-sheng2*. Quantitative Analysis of Ethanol Based on Laser Raman Spectroscopy Normalization Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3820-3825. |
[3] |
LIU Liang-yu, YIN Zuo-wei*, XU Feng-shun. Spectral Characteristics and Genesis Analysis of Gem-Grade Analcime From Daye, Hubei[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2799-2804. |
[4] |
LIN Jing-tao, XIN Chen-xing, LI Yan*. Spectral Characteristics of “Trapiche-Like Sapphire” From ChangLe, Shandong Province[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1199-1204. |
[5] |
LIU Rong1, 2, WANG Miao-miao1, 2 , SUN Ze-yu1, 2, CHEN Wen-liang1, 2, LI Chen-xi2*, XU Ke-xin1, 2. Research on Temperature Disturbance of Glucose Solution With
Two-Trace Two-Dimensional Correlation Spectrum Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1051-1055. |
[6] |
OU Li-juan1*, LI Jing1, ZHANG Chao-qun1, LUO Jian-xin1, WEI Ji1, WANG Hai-bo2*, ZHANG Chun-yan1. Redox-Controlled Turn-on Fluorescence Sensor for H2O2 and Glucose Using DNA-Template Gold Nanoclusters[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(12): 3757-3761. |
[7] |
MA Ping1, 2, Andy Hsitien Shen1*, LUO Heng1, ZHONG Yuan1. Study on Laser Raman Spectrum Characteristics of Jadeite From Common Origins[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(11): 3441-3447. |
[8] |
YAN Fang, ZHANG Jun-lin*, MAO Li-cheng, LIU Tong-hua, JIN Bo-yang. Research on Information Extraction Method of Carbohydrate Isomers Based on Terahertz Radiation[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(01): 26-30. |
[9] |
FU Xing-hu, ZHAO Fei, WANG Zhen-xing, LU Xin, FU Guang-wei, JIN Wa, BI Wei-hong. Quantitative Analysis of Goat Serum Protein Content by Raman Spectroscopy Based on IABC-SVR[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(02): 540-545. |
[10] |
LIN Xiao-mei, TAO Si-yu, LIN Jing-jun*, HUANG Yu-tao, CHE Chang-jin, SUN Hao-ran. Study on Improving the Stability of Heavy Metal Cu in Soil by Image Optimization[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(10): 3282-3286. |
[11] |
CHEN Quan-li1, WANG Hai-tao2*, LIU Xian-yu3, QIN Chen1, BAO De-qing1. Study on Gemology Characteristics of the Turquoise from Mongolia[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(07): 2164-2169. |
[12] |
LIN Xiao-mei1, HUANG Yu-tao1, LIN Jing-jun2*, TAO Si-yu1, CHE Chang-jin1. Quantitative Analysis of Soil Heavy Metals Based on LSSVM[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(05): 1523-1527. |
[13] |
LI Jia-jia1*, LIU Jing-li1, JIN Ru-yi1, TANG Yu-ping1, YUE Shi-jun1,WANG Li-wen2, LONG Xu1, ZHANG Guang-hui1, MENG Qing-hua1, LI Rong-xi3. Quantitative Measurement of Artemisinin Content in Chinese Traditional Compound Medicine by Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(08): 2403-2408. |
[14] |
ZHANG Yan-jun1, 2, ZHANG Fang-cao1, FU Xing-hu1*, JIN Pei-jun1, HOU Jiao-ru1. Detection of Fatty Acid Content in Mixed Oil by Raman Spectroscopy Based on ABC-SVR Algorithm[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(07): 2147-2152. |
[15] |
CHEN Tao, CAI Zhi-hua, HU Fang-rong, YIN Xian-hua, XU Chuan-pei*. A Study of Terahertz Spectra of Monosaccharides and Disaccharides with Structural Similarities[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(03): 686-692. |
|
|
|
|