| 光谱学与光谱分析 |
|
|
|
|
|
| The SERS Detection of SudanⅠby Using AAO as Template to Prepare the Substrate |
| PAN Xiao-hui, ZHANG Qin*, GUO Wei, CHEN Fa-he* |
| College of Food and Bioengineering, Jimei University, Fujian Provincial Key Laboratory of Food Microbiology and Enzyme Engineering, Xiamen 361021, China |
|
|
|
|
Abstract The large-scale controllable, ordered two-dimensional arrays of gold nanostructure with hot-spot were prepared together with chemical molecules were modified on the surface to concentrate SudanⅠwithin the zone of the SERS effect, which lead to analytical detection of SudanⅠin high resolution. The vapor of gold was deposed on anodic aluminum oxide(AAO)template by ～200 nm thickness to replicate its nanochannels, and the negative structure i.e. large-scale ordered gold nano-hemisphere array, was obtained after the removal of the template of AAO by NaOH solution. Au nano-hemisphere array was modified by 1-Dodecanethiol which can be self-assembled monolayer on the surface and concentrate SudanⅠwithin the zone of the SERS detection, which can facilitate the measurement of SudanⅠ. Due to the order and regularity of Au nano-hemisphere array, the signal of SudanⅠin the range of laser illumination is stable and uniform, and the quantitative analysis of SudanⅠwas realized. The SERS intensity of SudanⅠis logistic proportional to the concentration in the range of 10-7 to 5×10-4mol·L-1. The corresponding correlation coefficient of the liner equation is 0.99, the recoveries of SudanⅠare between 77%～117%. The limit of detection for SudanⅠis 4×10-8mol·L-1, comparable to that of HPLC of Chinese national standard method.
|
|
Received: 2014-05-14
Accepted: 2014-08-14
|
|
|
|
Corresponding Authors:
ZHANG Qin, CHEN Fa-he
E-mail: qinzhang@jmu.edu.cn;fhchen@jmu.edu.cn
|
|
[1] Refat A，Ibrahim Z S，Moustafa G G，et al. Journal of Biochemical and Molecular Toxicology，2008，22(2)：77.
[2] Qiao J D，Yan H Y，Wang H，et al. Chromatographia，2011，73(3/4)：227.
[3] Yan H Y，Wang H，Qian J D，et al. Journal of Chromatography A，2011，1218(16)：2182.
[4] Sun S，Wang Y，Yu W Z，et al. Journal of Separation Science，2011，34(14)：1730.
[5] Stiborova V，Martinek V，Rydlova H，et al. The Journal of Cancer Research，2002，62：5678.
[6] European Commission. Health and Consumer Protection Directorate General，Committee Ⅳ-Food Safety in Production and Currency，PartⅢPhysical and Chemical Substances Surveillance，New Method Declaration，1999.
[7] Xu Z，Wang S，Fang G，et al. Chromatographia，2010，71(5/6)：397.
[8] GB/T19681—2005. Beijing：China Standard Press (北京：中国标准出版社)，2005.
[9] Calbiani F，Careri M，Elviri L，et al. Journal of Chromatography A，2004，1042(1/2)：123.
[10] Rebane R，Leito I，Yurchenko S，et al. Journal of Chromatography A，2010，1217(17)：2747.
[11] Cornet V，Govaert Y，Moens G，et al. Journal of Agricultural and Food Chemistry，2006，54(3)：639.
[12] Di Anibal C V，Marsal L F，Callao M P，et al. Spectrochim Acta A，2012，87(2)：135.
[13] Wang H H，Liu C Y，Wu S B，et al. Advanced Materials，2006，18(4)：494.
[14] Nie S，Emory S R. Science，1997，275(5303)：1102.
[15] Sawai Y，Takimoto B，Nabika H，et al. Journal of American Chemical Society, 2007，129(6)：1658.
[16] Lee S J，Guan Z Q，Xu H X，et al. Journal of Physical Chemistry C, 2007，111(49)：17985.
[17] Haynes C L，Van Duyne R P. Journal of Physical Chemistry B，2001，105(24)：5599.
[18] Schierhorn M，Lee S J，Boettcher S W，et al. Advanced Materials，2006，18：2829.
[19] Foss C A，Hornyak G L，Stockert J A，et al. Journal of Physical Chemistry，1994，98，2963.
[20] Hornyak G L，Patrissi C J，Martin C R. Journal of Physical Chemistry B，1997，101(9)：1548.
[21] Lin H Y，Shao Q，Hu F，et al. Thin Solid Films，2012，526，133.
[22] Shao Q，Que R H，Cheng L，et al. The Royal Society of Chemistry，2012，2，1762.
[23] Shao Q，Que R H，Shao M W，et al. Advanced Functional Materials，2012，22(10)：2067.
[24] Que R H，Shao M W，Zhuo S J，et al. Advanced Functional Materials，2011，21(17)：3337.
[25] Si M Z，Kang Y P，Liu R M. Applied Surface Science，2012，258(15)：5533.
[26] Zhang M L，Fan X，Zhou H W，et al. Journal of Physical Chemistry，2010，114(5)：1969.
[27] Salmen R，Malterud K E，Pedersen B F. Acta Chemica Scandinavica，1988，42：493.
[28] Olivieri A C，Wilson R B，Paul I C，et al. Journal of Physical Chemistry C，2010，114(16)：7285.
[29] Munro C H，Smith W E，Armstrong D R，et al. Journal of Physical Chemistry，1995，99：879.
[30] Kunov-Kruse A J，Kristensen S B，Liu C，et al. Journal of Raman Spectroscopy，2011，42(6)：1470.
[31] Morant C，Marquez F，Campo T，et al. Thin Solid Films，2010，518(23)：6799.
[32] XIAO Hai-bo，ZHANG Qin，GUO Wei，et al(肖海波，张 芹，郭 伟，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2012，32(8)：2147.
[33] Bryant M A，Pemberton J E. Journal of the American Chemical Society，1991，113(22)：8284.
[34] Jiang X H，Lai Y C，Yang M，et al. Analyst，2012，137，3995.
[35] Kneipp J，Kenipp H，Kneipp K. Chemical Society Reviews，2008，37，1052. |
| [1] |
LAI Chun-hong*, ZHANG Zhi-jun, WEN Jing, ZENG Cheng, ZHANG Qi. Research Progress in Long-Range Detection of Surface-Enhanced Raman Scattering Signals[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(08): 2325-2332. |
| [2] |
LI Jia-jia, XU Da-peng *, WANG Zi-xiong, ZHANG Tong. Research Progress on Enhancement Mechanism of Surface-Enhanced Raman Scattering of Nanomaterials[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(05): 1340-1350. |
| [3] |
SUN Zhi-ming1, LI Hui1, FENG Yi-bo1, GAO Yu-hang1, PEI Jia-huan1, CHANG Li1, LUO Yun-jing1, ZOU Ming-qiang2*, WANG Cong1*. Surface Charge Regulation of Single Sites Improves the Sensitivity of
Raman Detection[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1075-1082. |
| [4] |
YIN Xiong-yi1, SHI Yuan-bo1*, WANG Sheng-jun2, JIAO Xian-he2, KONG Xian-ming2. Quantitative Analysis of Polycyclic Aromatic Hydrocarbons by Raman Spectroscopy Based on ML-PCA-BP Model[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 861-866. |
| [5] |
SUN Nan, TAN Hong-lin*, ZHANG Zheng-dong, REN Xiang, ZHOU Yan, LIU Jian-qi, CAI Xiao-ming, CAI Jin-ming. Raman Spectroscopy Analysis and Formation Mechanism of Carbon
Nanotubes Doped Polyacrylonitrile/Copper Cyclized to Graphite
at Room Temperature[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(09): 2983-2988. |
| [6] |
WANG Zi-xiong, XU Da-peng*, ZHANG Yi-fan, LI Jia-jia. Research Progress of Surface-Enhanced Raman Scattering Detection Analyte Molecules[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(02): 341-349. |
| [7] |
WAN Xiao-ming1, 2, ZENG Wei-bin1, 2, LEI Mei1, 2, CHEN Tong-bin1, 2. Micro-Distribution of Elements and Speciation of Arsenic in the Sporangium of Pteris Vittata[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(02): 470-477. |
| [8] |
HUANG Hui1, 2, TIAN Yi2, ZHANG Meng-die1, 2, XU Tao-ran2, MU Da1*, CHEN Pei-pei2, 3*, CHU Wei-guo2, 3*. Design and Batchable Fabrication of High Performance 3D Nanostructure SERS Chips and Their Applications to Trace Mercury Ions Detection[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(12): 3782-3790. |
| [9] |
FU Xing-hu, WANG Zhen-xing, MA Shuang-yu, ZHAO Fei, LU Xin, FU Guang-wei, JIN Wa, BI Wei-hong. Preparation and Properties of Micro-Cavity Silver Modified Fiber SERS Probe[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(09): 2800-2806. |
| [10] |
GUI Bo1, 2, YANG Yu-dong1, ZHAO Qian1, 2, SHI Meng1, MAO Hai-yang1, 3*, WANG Wei-bing1, CHEN Da-peng1, 3. A SERS Substrate for On-Site Detection of Trace Pesticide Molecules Based on Parahydrophobic Nanostructures[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(08): 2499-2504. |
| [11] |
SUN Ning, CHEN Jun-fan, ZHANG Jie*, ZHU Yong. The Forming Mechanism of Surface Morphology of Nanostructures and Its Effect on Graphene Raman Spectra[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(06): 1821-1827. |
| [12] |
ZHANG Can, ZHANG Jie*, DOU Xin-yi, ZHU Yong. Connection of Absorption and Raman Enhancement Characteristics of Different Types of Ag Nanoparticles[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(06): 1816-1820. |
| [13] |
DOU Xin-yi, ZHANG Can, ZHANG Jie*. Effects of Process Parameters on Double Absorption Resonance Peaks of Au Nanoparticles[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(05): 1446-1451. |
| [14] |
ZHANG Lei, ZHANG Xia*, WENG Yi-jin, LIU Xiao. Preparation and Properties of Ag/PANI Multifunction Nanozymes[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(11): 3399-3403. |
| [15] |
TIAN Hui-yan1，LIU Yu1, HUANG Jiao-qi1, XIE Feng-xin1, HUANG Guo-rong1, LIAO Pu1, FU Wei-ling1, ZHANG Yang2*. Research Progress and Application of Surface-Enhanced Raman Scattering Technique in Nucleic Acid Detection[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(10): 3021-3028. |
|
|
|
|
