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| Characterization and Determination of Gold Nanoparticles by SP-ICP-MS |
| SUN Chuan-qiang, GONG Zi-shan, WANG Xiao-jun, YANG Ru, JIANG Xue-hui, WANG Yan* |
| Department of Precision Instrument and Opto-Electronics Engineering, Tianjin University, Tianjin 300072, China |
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Abstract The continuous development of nanotechnology requires more powerful nanoparticle characterization techniques. Single particle inductively coupled plasma mass spectrometry (SP-ICP-MS) is a new technique for nanoparticle detection in recent years. It can quickly provide researchers with information on nanoparticle size, size distribution, particle number concentration and element composition, with small interference for samples. In this paper, the factors influencing the detection of gold nanoparticles (AuNPs)by SP-ICP-MS were discussed, which include the setting of parameters of the instrument, such as dwell time, the influence of sample matrix, including salt-containing and carbon-containingmatrix, and the dissolved analytical elements. The detection limit of gold nanoparticles was 23 nm. The recoveries of AuNPs were measured by spiked recovery. The recoveries were 97.7% and 84.4% for Taihu Lake and Dongli Lake, respectively. Finally, some existing problems were discussed in nanoparticle detection by SP-ICP-MS.
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Received: 2017-08-10
Accepted: 2018-01-22
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Corresponding Authors:
WANG Yan
E-mail: wangyan@tju.edu.cn
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[1] Chuankrerkkul N, Sangsuk S. Journal of Metals, Materials and Minerals, 2008, 18: 75.
[2] Kessler R. Environmental Health Perspectives, 2011, 19：A120.
[3] Mudalige T K, Qu H, Linder S W. Analytical Chemistry, 2015, 87：7395.
[4] Vance M E, Kuiken T, Vejerano E P, et al. Beilstein Journal of Nanotechnology, 2015, 6：1769.
[5] Peters R, Herrera-Rivera Z, Undas A, et al. Journal of Analytical Atomic Spectromtry, 2015, 30：1274.
[6] Mackevica A, Olsson M E, Hansen S F. Journal of Hazardous Materials, 2017, 322：270.
[7] Cascio C, Geiss O, Franchini F, et al. Journal of Analytical Atomic Spectromtry, 2015, 30：1255.
[8] Weigel S, Peters R, Loeschner K, et al. Analytical and Bioanalytical Chemistry, 2017, 409：4839.
[9] Degueldre C, Favarger P Y. Colloids and Surfaces A: Physicochemical and Engineering Aspects, 2003, 217：137.
[10] Degueldre C, Favarger P Y. Talanta, 2004, 62：1051.
[11] Degueldre C, Favarger P Y, Bitea C. Analytica Chimica Acta, 2004, 518：137.
[12] Degueldre C, Favarger P Y, Rosse R, et al. Talanta, 2006, 68：623.
[13] Degueldre C, Favarger P Y, Wold S. Analytica Chimica Acta, 2006, 555：263.
[14] Laborda F, Jiménez-Lamana J, Bolea E, et al. Journal of Analytical Atomic Spectrometry, 2011, 26：1362.
[15] Laborda F, Jiménez-Lamana J, Bolea E, et al. Journal of Analytical Atomic Spectrometry, 2013, 28：1220.
[16] Laborda F, Bolea E, Jimenez-Lamana J. Analytical Chemistry, 2014, 86：2270.
[17] Laborda F, Bolea E, Cepria G, et al. Analytica Chimica Acta, 2016, 904：10.
[18] Lee S, Bi X, Reed R B, et al. Environmental Science & Technology, 2014, 48：10291.
[19] Telgmann L, Metcalfe C D, Hintelmann H. Journal of Analytical Atomic Spectrometry, 2014, 29：1265.
[20] Caballero-Díaz E, Pfeiffer C, Kastl L, et al. Particle & Particle Systems Characterization, 2013, 30：1079.
[21] Su S, Chen B, He M, et al. Talanta, 2014, 119：458.
[22] Zheng L N, Wang M, Wang B, et al. Talanta, 2013, 116：782.
[23] Zhang S, Han G, Xing Z, et al. Analytical Chemistry, 2014, 86：3541.
[24] Wang M, Zheng L N, Wang B, et al. Analytical Chemistry, 2014, 86：10252.
[25] Hu B, He M, Chen B. Analytical and Bioanalytical Chemistry, 2015, 407：2685.
[26] Roman M, Rigo C, Castillo-Michel H, et al. Analytical and Bioanalytical Chemistry, 2015, 408：5109.
[27] Hsu K C, Hsu P F, Hung C C, et al. Talanta, 2017, 162：523.
[28] Montano M D, Olesik J W, Barber A G, et al. Analytical and Bioanalytical Chemistry, 2016, 408：5053.
[29] Bendall S C, Simonds E F, Qiu P, et al. Science, 2011, 332：687.
[30] Agatemor C, Beauchemin D. Analytica Chimica Acta, 2011, 706：66.
[31] Gajek R, Choe K Y. Journal of Analytical Atomic Spectrometry, 2015, 30：1142.
[32] Hineman A, Stephan C. Journal of Analytical Atomic Spectrometry, 2014, 29：1252. |
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