光谱学与光谱分析 |
|
|
|
|
|
Study on the Enhanced Spectrum Quantitative Analysis of SDBS Induced by β-Cyclodextrin |
SHI Dong-po, YIN Xian-qing, ZHENG Yan-cheng, CHEN Wu, FU Jia-xin, REN Zhao-hua |
College of Chemistry and Environmental Engineering, Yangtze University, Jingzhou 434023, China |
|
|
Abstract A novel enhanced ultraviolet absorption spectrometry method was developed for the quantitative analysis of SDBS induced by β-cyclodextrin(β-CD) with strong interferences. The ultraviolet absorption spectra of SDBS indicated that the presence of β-CD could result in the enhancement of absorption intensities of SDBS. A good linearity was obtained between the UV-absorption intensity of the system and the concentration of SDBS. The results indicated that the determination precision and the determination ranges of SDBS could be greatly improved by β-CD. The effect of several common interfering substances(SDS, OP-10, HPAM) on the determination of SDBS could be significantly reduced in β-CD aqueous solution. Therefore, the maximum errors of the determined SDBS were less than 2.0% under multifactor interferences, and the precision of the method was also as high as 10-2~10-3 mg·L-1. The stable inclusion of β-CD and SDBS could be automatically formed in water with molar ratio of 1:1. The stability constant of the inclusion, Ka, was 87 and the standard Gibbs function of molar reaction, ΔγGmΘ(298 K), was -11.064 kJ·mol-1. FTIR analysis exhibited that SDBS could be induced by β-CD since the phenyl group in SDBS molecule could exist stably in the cavity of β-CD and form the inclusion.
|
Received: 2012-12-21
Accepted: 2013-03-10
|
|
Corresponding Authors:
SHI Dong-po
E-mail: shidongpo2006@126.com
|
|
[1] Cantarero S, Camino-Sánchez F J, Zafra-Gómez A, et al. Marine Pollution Bulletin, 2012, 64(3): 587. [2] He X B, Guvench O, Mackerell A D Jr, et al. The Journal of Physical Chemistry B, 2010, 114 (30): 9787. [3] Inceoglua O, Sablayrollesb C, Van Elsasa J D, et al. Applied Soil Ecology, 2013, 63: 78. [4] Nimer M, Ballesteros O, Navalón A, et al. Analytical and Bioanalytical Chemistry, 2007, 387(6): 2175. [5] Dolenko S A, Alekseenko E Yu, Kuschevskaya N F. Journal of Analytical Chemistry, 2010, 65(3): 229. [6] Jullian C, Brossard V, Gonzalez I, et al. Journal of Solution Chemistry, 2011, 40(4): 727. [7] Zhang M F, Fu L, Wang J, et al. Journal of Photochemistry and Photobiology A: Chemistry, 2012, 228(1): 28. [8] Stachowicz A, Styrcz A, Korchowiec J, et al. Theoretical Chemistry Accounts: Theory, Computation, and Modeling, 2011, 130(4-6): 939. [9] Sudha N, Enoch I M V. Journal of Solution Chemistry, 2011, 40(10): 1755. [10] Maddens T, Vélaz I, Machín R, et al. Journal of Inclusion Phenomena and Macrocyclic Chemistry, 2011, 70(3-4): 415. [11] Abdel-Shafi A A, Al-Shihry S S. Journal of Inclusion Phenomena and Macrocyclic Chemistry, 2010, 67(1-2): 7. [12] Aigner Z, Berkesi O, Farkas G, et al. Journal of Pharmaceutical and Biomedical Analysis, 2012, 57: 62. [13] SHI Dong-po, JI Hong-bing, HU Xiao-fang, et al(石东坡, 纪红兵, 胡晓芳, 等). Journal of Chemical Engineering of Chinese Universities(高校化学工程学报), 2007, 21(3): 460. [14] Neoh T L, Yamamoto C, Ikefuji S, et al. Food Chemistry, 2012, 131(4): 1123. [15] Shi D P, Ji H B. Chinese Chemical Letters, 2009, 20(2): 139. |
[1] |
LIU Hao-dong1, 2, JIANG Xi-quan1, 2, NIU Hao1, 2, LIU Yu-bo1, LI Hui2, LIU Yuan2, Wei Zhang2, LI Lu-yan1, CHEN Ting1,ZHAO Yan-jie1*,NI Jia-sheng2*. Quantitative Analysis of Ethanol Based on Laser Raman Spectroscopy Normalization Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3820-3825. |
[2] |
LIN Hong-jian1, ZHAI Juan1*, LAI Wan-chang1, ZENG Chen-hao1, 2, ZHAO Zi-qi1, SHI Jie1, ZHOU Jin-ge1. Determination of Mn, Co, Ni in Ternary Cathode Materials With
Homologous Correction EDXRF Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(11): 3436-3444. |
[3] |
HUANG Li, MA Rui-jun*, CHEN Yu*, CAI Xiang, YAN Zhen-feng, TANG Hao, LI Yan-fen. Experimental Study on Rapid Detection of Various Organophosphorus Pesticides in Water by UV-Vis Spectroscopy and Parallel Factor Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(11): 3452-3460. |
[4] |
LI Zhong-bing1, 2, JIANG Chuan-dong2, LIANG Hai-bo3, DUAN Hong-ming2, PANG Wei2. Rough and Fine Selection Strategy Binary Gray Wolf Optimization
Algorithm for Infrared Spectral Feature Selection[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3067-3074. |
[5] |
LIU Shu1, JIN Yue1, 2, SU Piao1, 2, MIN Hong1, AN Ya-rui2, WU Xiao-hong1*. Determination of Calcium, Magnesium, Aluminium and Silicon Content in Iron Ore Using Laser-Induced Breakdown Spectroscopy Assisted by Variable Importance-Back Propagation Artificial Neural Networks[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3132-3142. |
[6] |
KONG De-ming1, LIU Ya-ru1, DU Ya-xin2, CUI Yao-yao2. Oil Film Thickness Detection Based on IRF-IVSO Wavelength Optimization Combined With LIF Technology[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2811-2817. |
[7] |
ZHAO Yu-wen1, ZHANG Ze-shuai1, ZHU Xiao-ying1, WANG Hai-xia1, 2*, LI Zheng1, 2, LU Hong-wei3, XI Meng3. Application Strategies of Surface-Enhanced Raman Spectroscopy in Simultaneous Detection of Multiple Pathogens[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2012-2018. |
[8] |
CHENG Xiao-xiang1, WU Na2, LIU Wei2*, WANG Ke-qing2, LI Chen-yuan1, CHEN Kun-long1, LI Yan-xiang1*. Research on Quantitative Model of Corrosion Products of Iron Artefacts Based on Raman Spectroscopic Imaging[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2166-2173. |
[9] |
CHEN Rui1, WANG Xue1, 2*, WANG Zi-wen1, QU Hao1, MA Tie-min1, CHEN Zheng-guang1, GAO Rui3. Wavelength Selection Method of Near-Infrared Spectrum Based on
Random Forest Feature Importance and Interval Partial
Least Square Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1043-1050. |
[10] |
DENG Xiao-jun1, 2, MA Jin-ge1, YANG Qiao-ling3, SHI Yi-yin1, HUO Yi-hui1, GU Shu-qing1, GUO De-hua1, DING Tao4, YU Yong-ai5, ZHANG Feng6. Visualized Fast Identification Method of Imported Olive Oil Quality Grade Based on Raman-UV-Visible Fusion Spectroscopy Technology[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1117-1125. |
[11] |
WANG Hai-ping1, 2, ZHANG Peng-fei1, XU Zhuo-pin1, CHENG Wei-min1, 3, LI Xiao-hong1, 3, ZHAN Yue1, WU Yue-jin1, WANG Qi1*. Quantitative Determination of Na and Fe in Sorghum by LIBS Combined With VDPSO-CMW Algorithm[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 823-829. |
[12] |
XU Wei-xin, XIA Jing-jing, WEI Yun, CHEN Yue-yao, MAO Xin-ran, MIN Shun-geng*, XIONG Yan-mei*. Rapid Determination of Oxytetracycline Hydrochloride Illegally Added in Cattle Premix by ATR-FTIR[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 842-847. |
[13] |
ZHENG Li-na1, 2, XUAN Peng1, HUANG Jing1, LI Jia-lin1. Development and Application of Spark-Induced Breakdown Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 665-673. |
[14] |
GAO Xi-ya1, 2, 3, ZHANG Zhu-shan-ying1, 2, 3*, LU Cui-cui1, 2, 3, MENG Yong-ji1, 2, 3, CAO Hui-min1, 2, 3, ZHENG Dong-yun1, 2, 3, ZHANG Li1, 2, 3, XIE Qin-lan1, 2, 3. Quantitative Analysis of Hemoglobin Based on SiPLS-SPA
Wavelength Optimization[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(01): 50-56. |
[15] |
LI Yuan1, ZHANG Wen-bo1, CHEN Xiao-lin2, 3, LI Han1, ZHANG Guan-jun1. Application of Gaussian Process Regression on the Quantitative Analysis of the Aging Condition of Insulating Paper by Near-Infrared Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3073-3078. |
|
|
|
|