| 光谱学与光谱分析 |
|
|
|
|
|
| Analytical Method for On-Site Test of Drug Precursor Chemicals |
| YOU Xiao-ming, HONG Li-jun*, LI Zhi-hao, SHU Tian-min |
| The Third Research Institute of The Ministry of Public Security of P.R.C., Shanghai 200031, China |
|
|
|
|
Abstract Thirteen kinds of common drug precursor chemicals were detected on the spot by transportable Raman spectrometer independently researched and developed. Changing analysis methods, such as the focal position of the instrument, analysis time, external light source, sample containers and the concentration of the analyte, the high quality Raman spectrums were obtained. The study shows that analysis method can be optimized to improve the detection efficiency, LOD(limit of detection)of 1-phenyl-2-acetone, toluene and chloroform was recorded for lower concentrations and the component contents of the mixture have a significant impact on the test results. Selecting the appropriate instrument conditions can be more effective and fast screening of precursor chemicals on site to provide help for those who are engaged in the anti-drug work．
|
|
Received: 2012-07-23
Accepted: 2012-11-30
|
|
|
|
Corresponding Authors:
HONG Li-jun
E-mail: hong6450@yeah.net
|
|
[1] Kankaanpas A，Gunnar T，Ariniemi K. J. Chromatogr. B，2004，810(1): 57.
[2] Meng Q，Cepeda M，Kramer T. J. Chromatogr. B，2000，721(1): 115.
[3] Cheng P S，Fu C Y，Lee C H. J. Chromatorgr B，2007，852(1): 443.
[4] Vergote G J，Vervaet C J，Remon P，et al. Eur. J. Pharmacol.，2002，16: 63.
[5] WEI Wan-zhi，HU Yan-bo，XIA Jian-jun，et al(魏万之, 胡妍波, 夏建军, 等). Journal of Hunan University: Natural Sciences(湖南大学学报·自然科学版)，2005，32(2): 76.
[6] YANG Jia-hong，GAN Feng，LIANG Yi-zeng，et al(杨家红，甘 峰，梁逸曾，等). Jonrnal of Hunan University: Natural Sciences(湖南大学学报·自然科学版)，2001，28(1): 37.
[7] Tsuchihashi H，Katagi M，Nishikawa M，et al. Appl. Spectrosc.，1997，51(12): 1796.
[8] Ryder A G，O’Connor G M，Glynn T J. J. Raman Spectrosc.，2000，31(3): 221.
[9] Vandenabeele P，Castro K，Hargreaves M，et al. Anal. Chim. Acta，2007，588: 108.
[10] Lewis M L，Lewis I R，Griffiths P R. Vib. Spectrosc.，2005，38: 11.
[11] Hargreaves M D，Page K，Munschi T，et al. J. Raman Spectrosc.，2008，39: 873. |
| [1] |
LI Jie, ZHOU Qu*, JIA Lu-fen, CUI Xiao-sen. Comparative Study on Detection Methods of Furfural in Transformer Oil Based on IR and Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 125-133. |
| [2] |
WANG Fang-yuan1, 2, HAN Sen1, 2, YE Song1, 2, YIN Shan1, 2, LI Shu1, 2, WANG Xin-qiang1, 2*. A DFT Method to Study the Structure and Raman Spectra of Lignin
Monomer and Dimer[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 76-81. |
| [3] |
XING Hai-bo1, ZHENG Bo-wen1, LI Xin-yue1, HUANG Bo-tao2, XIANG Xiao2, HU Xiao-jun1*. Colorimetric and SERS Dual-Channel Sensing Detection of Pyrene in
Water[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 95-102. |
| [4] |
WANG Xin-qiang1, 3, CHU Pei-zhu1, 3, XIONG Wei2, 4, YE Song1, 3, GAN Yong-ying1, 3, ZHANG Wen-tao1, 3, LI Shu1, 3, WANG Fang-yuan1, 3*. Study on Monomer Simulation of Cellulose Raman Spectrum[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 164-168. |
| [5] |
WANG Lan-hua1, 2, CHEN Yi-lin1*, FU Xue-hai1, JIAN Kuo3, YANG Tian-yu1, 2, ZHANG Bo1, 4, HONG Yong1, WANG Wen-feng1. Comparative Study on Maceral Composition and Raman Spectroscopy of Jet From Fushun City, Liaoning Province and Jimsar County, Xinjiang Province[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 292-300. |
| [6] |
LI Wei1, TAN Feng2*, ZHANG Wei1, GAO Lu-si3, LI Jin-shan4. Application of Improved Random Frog Algorithm in Fast Identification of Soybean Varieties[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3763-3769. |
| [7] |
WANG Zhi-qiang1, CHENG Yan-xin1, ZHANG Rui-ting1, MA Lin1, GAO Peng1, LIN Ke1, 2*. Rapid Detection and Analysis of Chinese Liquor Quality by Raman
Spectroscopy Combined With Fluorescence Background[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3770-3774. |
| [8] |
LIU Hao-dong1, 2, JIANG Xi-quan1, 2, NIU Hao1, 2, LIU Yu-bo1, LI Hui2, LIU Yuan2, Wei Zhang2, LI Lu-yan1, CHEN Ting1，ZHAO Yan-jie1*，NI Jia-sheng2*. Quantitative Analysis of Ethanol Based on Laser Raman Spectroscopy Normalization Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3820-3825. |
| [9] |
LU Wen-jing, FANG Ya-ping, LIN Tai-feng, WANG Hui-qin, ZHENG Da-wei, ZHANG Ping*. Rapid Identification of the Raman Phenotypes of Breast Cancer Cell
Derived Exosomes and the Relationship With Maternal Cells[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3840-3846. |
| [10] |
LI Qi-chen1, 2, LI Min-zan1, 2*, YANG Wei2, 3, SUN Hong2, 3, ZHANG Yao1, 3. Quantitative Analysis of Water-Soluble Phosphorous Based on Raman
Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3871-3876. |
| [11] |
GUO He-yuanxi1, LI Li-jun1*, FENG Jun1, 2*, LIN Xin1, LI Rui1. A SERS-Aptsensor for Detection of Chloramphenicol Based on DNA Hybridization Indicator and Silver Nanorod Array Chip[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(11): 3445-3451. |
| [12] |
ZHU Hua-dong1, 2, 3, ZHANG Si-qi1, 2, 3, TANG Chun-jie1, 2, 3. Research and Application of On-Line Analysis of CO2 and H2S in Natural Gas Feed Gas by Laser Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(11): 3551-3558. |
| [13] |
LIU Jia-ru1, SHEN Gui-yun2, HE Jian-bin2, GUO Hong1*. Research on Materials and Technology of Pingyuan Princess Tomb of Liao Dynasty[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(11): 3469-3474. |
| [14] |
LI Wen-wen1, 2, LONG Chang-jiang1, 2, 4*, LI Shan-jun1, 2, 3, 4, CHEN Hong1, 2, 4. Detection of Mixed Pesticide Residues of Prochloraz and Imazalil in
Citrus Epidermis by Surface Enhanced Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3052-3058. |
| [15] |
ZHAO Ling-yi1, 2, YANG Xi3, WEI Yi4, YANG Rui-qin1, 2*, ZHAO Qian4, ZHANG Hong-wen4, CAI Wei-ping4. SERS Detection and Efficient Identification of Heroin and Its Metabolites Based on Au/SiO2 Composite Nanosphere Array[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3150-3157. |
|
|
|
|
