光谱学与光谱分析 |
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Study of the Raman-AFM System for Simultaneous Measurements of Raman Spectrum and Micro/Nano-Structures |
SHI Bin, ZHANG Hai-jun, WU Lan, ZHANG Dong-xian* |
State Key Laboratory of Modern Optical Instruments, Zhejiang University, Hangzhou 310027, China |
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Abstract This paper proposes a novel technique of Raman-atomic force microscopy (AFM) combining micro region Raman spectroscopy and AFM imaging. An in-situ probe unit which can simultaneously realize the detection of Raman spectrum and the measurement of AFM image was designed, and a related Raman-AFM system was constructed. Using this system, some experiments were carried out to acquire micro region Raman spectra and AFM images of ZnO nano-particle and TiO2 film. The results show that the Raman spectra of both samples are in agreement with theoretical vaues, and the AFM images represent their micro/nano-structures quite well. These researches prove the feasibility of the Raman-AFM technique which has the potential of being widely applied in the fields of Raman spectroscopy and micro/nano-technology.
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Received: 2011-08-11
Accepted: 2011-11-28
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Corresponding Authors:
ZHANG Dong-xian
E-mail: zhangdx@zju.edu.cn
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[1] Filik Jacob. Spectroscopy Europe, 2005, 17(5): 10. [2] Manish S, Nidih V, Animesh K. Ojha. Vibrational Spectroscopy, 2011, 56(1): 19. [3] Huang Y Y, Beal CM, Cai W W, et al. Biotechnology and Bioengineering, 2009, 99: 1. [4] Binnig G, Quate C F. Physical Review Letters, 1986, 56(5): 930. [5] Wolf J F, Hillner P E, Bilewicz R, et al. Review of Scientific Instruments, 1999, 70(6): 2751. [6] Creely C M, Singh G P, Petrov D. Optics Communications, 2005, 245: 465. [7] Sharma S K, Misra A K, Luecy P G, et al. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy, 2009, 73(3): 468. [8] Garcia-Vidal F J, Pendry J B. Physical Review Letters, 1996, 77(6): 1163. [9] Frost R L, Weier M, Martens W, et al. Mineralogical Magazine, 2005, 69(2): 169. [10] Futamata, Masayuki. Analytical Sciences, 2001, 17: 693. [11] Bizzarri A R, Cannistraro S. Analytical Biochemistry, 2009, 293: 149. [12] Yoon M J. Journal of the Chinese Chemical Society, 2009, 56: 443. [13] Fu X, Zhang D X, Zhang H J. Chinese Optics Letters, 2009, 7(10): 891. [14] Wang X, Zhang D, Zhang H, et al. Nanotechnology, 2011, 22: 305306. [15] Damen T C, Porto S P S, Tell B. Physics Review, 1966, 142: 570. [16] Choi C H, Jung Y M, Kim S B. Vibrational Spectroscopy, 2005, 37: 33. |
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