Advance of Development and Application of GC-IR Technology
HUANG Yi-fei1, CAI Zan2, HU Jing1, LIN Li-qiong2, XIAO Xiao-hua2*, LI Gong-ke2*
1. China Tobacco Guangdong Industrial Co, Ltd., Guangzhou 510000, China 2. School of Chemistry and Chemical Engineering, Sun Yat-sen University, Guangzhou 510275, China
Abstract:The gas chromatograph (GC)-infrared spectroscopy (IR) technique combines the particular separating capacity of GC and the faultlessly with distinguishing capacity of molecular structure of IR, its detective sensitivity is very high and itis used to separate and identify many kinds of complicated compounds from element speciation analysis, natural products, and gasoline. This paper introduces the principle of GC-IR. Three types of interface techniques, light pipe technique, matrix isolation technique and direct deposition technique are compared. Connection type with other detections and factors influencing sensitivity in interface are also introduced. The improvement and achievement in coupling GC system, interface, data processing techniques and its application is reviewed in the present paper.
黄翼飞1,蔡 赞2,胡 静1,林丽琼2,肖小华2*,李攻科2* . 气相色谱-红外光谱联用技术及应用研究进展 [J]. 光谱学与光谱分析, 2015, 35(08): 2130-2135.
HUANG Yi-fei1, CAI Zan2, HU Jing1, LIN Li-qiong2, XIAO Xiao-hua2*, LI Gong-ke2* . Advance of Development and Application of GC-IR Technology . SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(08): 2130-2135.
[1] Zhang L, Zeng Z, Zhao C, et al. Journal of Chromatography A, 2013, 1313: 245. [2] Cherta L, Portolés T, Beltran J, et al. Journal of Chromatography A, 2013, 1314: 224. [3] Grabowska-Polanowska B, Faber J, Skowron M, et al. Journal of Chromatography A, 2013, 1301: 179. [4] Schneider J F, Demirgian J C, Stickler J C. Journal of Chromatographic Science, 1986, 24(8): 330. [5] Anderson K B, Tranter R S, Tang W, et al. The Journal of Physical Chemistry A, 2004, 108(16): 3403. [6] Bourne S, Haefner A M, Norton K L, et al. Analytical Chemistry, 1990, 62(22): 2448. [7] LIU Shi-lei, XU Da-nian(刘石磊,许大年). Modern Scientific Instruments(现代科学仪器), 2005, (04): 47. [8] FANG Zhi, YU Gang, ZHOU Zheng(方 智,于 刚,周 铮). Chemical Analysis and Meterage(化学分析计量), 2013, 22(2): 57. [9] Gachot G, Grugeon S, Jimenez-Gordon I, et al. Analytical Methods, 2014, 6(15): 6120. [10] de Haseth J A, Isenhour T L. Analytical Chemistry, 1977, 49(13): 1977. [11] WANG Zheng-fan (汪正范). Hyphenated Chromatographic Techniques(色谱联用技术). Beijing: Chemical Industry Press(北京:化学工业出版社), 2007. 203. [12] SANG Wen-qiang, LI Jun, LIN Ping(桑文强,李 军,林 平). Flavour Fragrance Cosmetics(香料香精化妆品), 2003, (02): 7. [13] LIU Ying, HU Chang-qin(刘 颖,胡昌勤). Chinese Journal of Pharmaceutical Analysis(药物分析杂志), 2009, (03): 512. [14] ZHANG Le-feng, SONG Guo-nan, CHE Xun, et al (张乐沣,宋果男,车 迅,等). Chinese Journal of Chromatography (色谱), 1985, (S1): 121. [15] ZHONG Shan(钟 山). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 1995,15(6): 41. [16] Bombarda I, Dupuy N, Da J P L V, et al. Analytica Chimica Acta, 2008, 613(1): 31. [17] Praisler M, Ciochina S. Journal of Analytical Methods in Chemistry, 2014, 342497. [18] Mjos S A, Pettersen J. Journal of the American Oil Chemists’ Society, 2003, 80(9): 839. [19] Jones T H, Garraffo H M, Spande T F, et al. Journal of Natural Products, 2010, 73(3): 313. [20] XUE Hui-feng, ZHAO Jia-lin, LIU Man-cang, et al(薛慧峰, 赵家林, 刘满仓,等). Chinese Journal of Analytical Chemistry(分析化学), 2004, 32(9): 1145. [21] XUE Hui-feng, GENG Zhan-jie, QIN Peng, et al(薛慧峰,耿占杰,秦 鹏,等). Petrochemical Technology & Application(石化技术与应用), 2011(04): 362. [22] XUE Hui-feng, ZHAO Jia-lin, ZHAO Xu-tao, et al(薛慧峰,赵家林,赵旭涛,等). Chinese Journal of Analytical Chemistry(分析化学), 2006(S1): 141. [23] Kempe J, Bellmann C, Meyer D, et al. Analytical and Bioanalytical Chemistry, 2005, 382(1): 186. [24] FANG Li-na, CHEN Yu, LIU Ya, et al(方丽娜,陈 宇,刘 娅,等). Guangzhou Chemical Industry(广州化工), 2015,(06): 45. [25] WANG Qi, WANG Shu-rong, WANG Le, et al(王 琦,王树荣,王 乐,等). Journal of Engineering Thermophysics (工程热物理学报), 2007(01): 173. [26] TAN Hong, WANG Shu-rong, LUO Zhong-yang, et al(谭 洪,王树荣,骆仲泱,等). Journal of Agricultural Machinery(农业机械学报), 2005, 36(4): 30, 38. [27] LIANG Ming, XIAO Ting-ting, JIANG Xiao-li, et al(梁 鸣,肖婷婷,姜晓黎,等). Flavour Fragrance Cosmetics(香料香精化妆品), 2011,(02): 1. [28] LIANG Ming, CHEN Min, CAI Chun-ping(梁 鸣,陈 敏,蔡春平,等). Chinese Journal of Chromatography(色谱), 2002,(06): 577. [29] WANG Cheng-yun, GONG Li-wen, LI Jing-hui (王成云,龚丽雯,李京会). China Surfactant Detergent & Cosmetics(日用化学工业), 2004,(03): 187. [30] Takeoka Gary R, Buttery Ron G. Food Chemistry, 2012, 132(4): 2131. [31] LUO Li-mei, ZHANG Hua, JIN Kun, et al(罗丽梅,张 华,靳 焜,等). Chinese Journal of Spectroscopy Laboratory(光谱实验室), 2013,(05): 2067. [32] ZHANG Min(张 敏). Chinese Journal of Synthetic Chemistry(合成化学), 2006, 02: 143. [33] WU Lin, YI De-lian, QIN Xiao-rong, et al(伍 林,易德莲,秦晓蓉, 等). Journal of Wuhan University of Science and Technology(Natural Science Edition)(武汉科技大学学报·自然科学版), 2005, 02: 166. [34] Basiuk V A, Douda J. Journal of Analytical and Applied Pyrolysis, 2001, 60(1): 27. [35] Basiuk V A, Douda J. Journal of Analytical and Applied Pyrolysis, 2000, 55(2): 235. [36] Gonzalez A, Irusta L, Fernández-Berridi M J, et al. Polymer Degradation and Stability, 2005, 87(2): 347. [37] Awad T, Belal T, DeRuiter J, et al. Forensic Science International, 2009, 185(1): 67. [38] Awad T, Belal T, DeRuiter J, et al. Forensic Science International, 2010, 194(1): 39. [39] Maher H M, Awad T, Clark C R. Forensic Science International, 2009, 188(1): 31. [40] Abdel-Hay K M, Awad T, DeRuiter J, et al. Forensic Science International, 2010, 195(1): 78. [41] Abdel-Hay K M, DeRuiter J, Clark C R. Forensic Science International, 2013, 231(1-3): 54. [42] Chappell J S, Lee M M. Forensic Science International, 2010, 195(1): 108. [43] Gosav S, Praisler M, Birsa M L. International Journal of Molecular Sciences, 2011, 12(12): 6668. [44] YU Wan-ying, ZHANG Hua, HUANG Wei-dong, et al(于万滢,张 华,黄威东, 等). Chinese Journal of Chromatography(色谱), 2005, 02: 196. [45] Liu Y, Hu C. Analytica Chimica Acta, 2006, 575(2): 246. [46] Teal P E A, Jones D, Jones G, et al. Journal of Natural Products, 2014, 77(2): 402. [47] Lee H, Finckbeiner S, Yu J S, et al. Journal of Chromatography A, 2007, 1165(1-2): 136. [48] YAO Qiang, CHANG Tao, LIU Yong, et al(姚 强,常 涛,刘 永, 等). Journal of Chongqing University (Natural Science Edition)(重庆大学学报), 2009, 07: 798. [49] Garg P, Purohit A, Tak V K, et al. Journal of Chromatography A, 2009, 1216(45): 7906.