合金钢的激光诱导击穿光谱实验条件优化

doi:10.3964/j.issn.1000-0593(2013)02-0531-04

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摘要：利用1 064 nm波长Nd∶YAG脉冲激光诱导击穿合金钢产生激光等离子体光谱，采用高分辨率及门宽控制的ICCD探测LIBS信号光谱。选用铁元素原子谱线404.581，414.387，427.176和438.355 nm进行分析，研究了不同实验参数对LIBS光谱信号强度的影响结果。实验结果表明，激光脉冲能量、激光聚焦位置以及ICCD探测器的延时等实验参数对合金钢LIBS信号有较大影响。通过优化这些实验参数，获得高光谱强度和信背比的LIBS信号，确定了LIBS技术用于合金钢微量元素成分分析的最佳实验条件，从而开展合金钢样品成分分析。

关键词：激光诱导击穿光谱;光谱强度;信背比;合金钢

Abstract：Laser induced plasma spectroscopy of alloy steel was produced by Nd∶YAG pulsed laser at 1 064 nm, and the spectral signal was detected by high resolution and width controlled ICCD. Several Fe atomic spectral lines such as 404.581, 414.387, 427.176 and 438.355 nm were chosen for analysis, and the effects of different experimental parameters on LIBS spectral signal intensity were investigated. It is shown that the experimental parameters such as pulse energy, laser focus location and laser delay time have great influence on the LIBS signal. LIBS signals with high spectral intensity and signal-background ratio (SBR) as well as the optimum experiment conditions were obtained by optimizing these experiment parameters so as to make composition analysis of the alloy steel.

Key words：LIBS;Spectral intensity;SBR;Alloy steel

收稿日期: 2012-06-29 修订日期: 2012-09-20

中图分类号:

O433.4

通讯作者: 高勋 E-mail: lasercust@yahoo.com.cn

引用本文:

邵妍，高勋^*，杜闯，赵振明，陈伟钰，郝作强，孙长凯，林景全 . 合金钢的激光诱导击穿光谱实验条件优化 [J]. 光谱学与光谱分析, 2013, 33(02): 531-534.
SHAO Yan, GAO Xun^*, DU Chuang, ZHAO Zhen-ming, CHEN Wei-yu, HAO Zuo-qiang, SUN Chang-kai, LIN Jing-quan . The LIBS Experiment Condition Optimization of Alloy Steel . SPECTROSCOPY AND SPECTRAL ANALYSIS, 2013, 33(02): 531-534.

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https://www.gpxygpfx.com/CN/10.3964/j.issn.1000-0593(2013)02-0531-04 或 https://www.gpxygpfx.com/CN/Y2013/V33/I02/531