光谱学与光谱分析
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可调谐半导体激光吸收光谱技术检测痕量乙烯气体的系统研制
潘卫东1 ,张佳薇2 ,戴景民1 ,宋 凯1
1. 哈尔滨工业大学电气工程及自动化学院,黑龙江 哈尔滨 150001 2. 东北林业大学机电工程学院,黑龙江 哈尔滨 150040
Tunable Diode Laser Absorption Spectroscopy System for Trace Ethylene Detection
PAN Wei-dong1 , ZHANG Jia-wei2 , DAI Jing-min1 , SONG Kai1
1. School of Electrical Engineering and Automation, Harbin Institute of Technology, Harbin 150001, China 2. College of Electromechanical Engineering, Northeast Forestry University, Harbin 150040, China
摘要 : 可调谐半导体激光吸收光谱技术(TDLAS)利用激光器的窄线宽和波长调谐特性,使其扫描被测气体的单个吸收峰,实现痕量气体的高分辨率、高灵敏度快速检测。通过分析近红外波段的乙烯吸收谱线特性,选取1 626.8 nm附近的吸收峰作为检测谱线,研制了基于white池结构的TDLAS检测系统,结合波长调制和二次谐波检测,对体积分数为20~1 200 ppmv的乙烯气体进行了测量,推算该系统的检测下限约为10 ppmv。
关键词 :TDLAS;乙烯;痕量气体;波长调制
Abstract :Tunable diode laser absorption spectroscopy (TDLAS) was characterized by ultra-narrow line width laser and wavelength modulation, which makes it possible to scan a single absorption line. TDLAS has an advantage in trace gas analysis for its high resolution, high sensitivity and quick response. The 1 626.8 nm absorption line of ethylene was selected for detecting by analyzing its absorption line characteristic. The TDLAS system was developed with a white type multi-pass cell, combined with wavelength modulation and harmonic detection. Ethylene concentration ranges from 20 to 1 200 ppmv were tested using this system. The estimated detection limit of the system is 10 ppmv.
Key words :TDLAS;Ethylene;Trace gas;Wavelength modulation
收稿日期: 2012-03-30
修订日期: 2012-06-25
通讯作者:
潘卫东
E-mail: whispe@163.com
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