In Vivo Determination of Pb in Human Bone by Using X-Ray Fluorescence Analysis
LUO Li-qiang1, XU Tao1, CHU Bin-bin1, SUN Jian-ling1, Egden L2, Chettle D2, WANG Xiao-fang1, BO Ying1, LIU Ying1, WANG Shu-xian1, TANG Li-jun1, LI Ying-chun1
1. National Research Center for Geoanalysis, Beijing 100037, China 2. McMaster University, Hamilton, Canada
Abstract：The data of in vivo XRF Pb in human bone were obtained within China by using the in vivo XRF set. The K series X-ray of Pb were applied to determine the in vivo Pb concentration in tibia and calcaneus among Chinese mainland residents. For general population, the weighted average of Pb in bone was 0.4～22.7 μg·(lead g bone mineral)-1. The uncertainty was 7.0～12.5 μg·(lead g bone mineral)-1, and the average minimun detection limit was 20.3μg·(lead g bone mineral)-1. For residents from pollution area, the maximum Pb in bone reached up to 73.9 μg·(lead g bone mineral)-1.
Key words：In vivo analysis;Lead in bone;X-ray fluorescence
罗立强1，许 涛1，储彬彬1，孙建伶1，Egden L2，Chettle D2，王晓芳1，伯 英1，刘 颖1，王淑贤1，唐力君1，李迎春1 . 原位活体骨铅X射线荧光光谱分析[J]. 光谱学与光谱分析, 2012, 32(03): 821-825.
LUO Li-qiang1, XU Tao1, CHU Bin-bin1, SUN Jian-ling1, Egden L2, Chettle D2, WANG Xiao-fang1, BO Ying1, LIU Ying1, WANG Shu-xian1, TANG Li-jun1, LI Ying-chun1 . In Vivo Determination of Pb in Human Bone by Using X-Ray Fluorescence Analysis . SPECTROSCOPY AND SPECTRAL ANALYSIS, 2012, 32(03): 821-825.
[1] Hoffer P B, Jones W B, Crawford R B, et al. Radiology, 1968, 90: 342. [2] Ahlgren L, Liden K, Mattson S, et al. Work Environ. & Health, 1976, 2: 82. [3] Bojesson J, Mattsson S. in X-ray Spectrometry: Recent Technological Advances. Tsuji K, Injuk J, Van Grieken R(eds), 2004. 487. [4] Chettle D R, Radioanal J. Nucl. Chem., 2006, 268(3): 653. [5] Parsons P J, Bellis D J, Hetter K M, et al. X-Ray Spectrometry, 2008, 37(1): 76. [6] McNeil F E, O’Meara J M. Adv. X-Ray Anal., 1999, 41: 910. [7] Gordon C L, Chettle D R, Webber C E, et al. Med., 1993, 50: 637. [8] Brito J A A, McNeil F E, Webber C E, et al. Environ. Monit., 2005, 7: 241. [9] Stewart W F, Schwartz B S, Simon D, et al. Environ. Health Persp., 2002, 110: 501. [10] Nie H, Chettle D, Stronach I, et al. Nuclear Instruments and Methods in Physics Research B, 2004, 213: 579. [11] LUO Li-qiang(罗立强). X-Ray Fluorescence Spectrometer(X射线荧光光谱仪). Beijing: Chemical Industry Press(北京：化学工业出版社)，2008. 11.
