Real-Time Monitoring of Industrial Acetic Acid Production Process Using a New Type of Online NIR Analysis System
YE Hua-jun1, 2, ZHANG Xue-feng2, WU Ji-ming2, XIA A-lin1, WANG Xin2, YANG Hui-hua3, WANG Jian1*
1. Electronic Information College, Hangzhou Dianzi University, Hangzhou 310018, China 2. Focused Photonics (Hangzhou), Inc., Hangzhou 310052, China 3. College of Computer and Control, Guilin University of Electronic Technology, Guilin 541004, China
Abstract:The safe and real-time monitoring of the production process of acetic acid is always a key technical problem. The conventional online chromatographic analysis can’t satisfy the requirements of real-time analysis for its inherent disadvantages. A new type of on-line near-infrared analysis system has been developed for real-time analysis of the concentration of each component in acetic acid reaction kettles instantly. Its features and configuration were described in detail. Both the laboratory modeling and field application results have confirmed that this system is of high stability and accuracy. The proposed system can effectively solve the key technical problems in the manufacture and ensure the safety and stability of production process of acetic acid.
叶华俊1, 2,张学锋2,吴继明2,夏阿林1,王 欣2,杨辉华3, 王 健1* . 新型在线近红外分析系统用于工业醋酸生产的实时监测 [J]. 光谱学与光谱分析, 2010, 30(05): 1234-1237.
YE Hua-jun1, 2, ZHANG Xue-feng2, WU Ji-ming2, XIA A-lin1, WANG Xin2, YANG Hui-hua3, WANG Jian1* . Real-Time Monitoring of Industrial Acetic Acid Production Process Using a New Type of Online NIR Analysis System . SPECTROSCOPY AND SPECTRAL ANALYSIS, 2010, 30(05): 1234-1237.
[1] 今日化工. 醋酸调研报告. http://www.todaychem.cn/Index.html. [2] LONG Jian-ping(龙建平). Guizhou Chemical Industry(贵州化工),2003,28:3. [3] ZONG Yan-gong(宗言恭). Chemical Industry(化学工业),1998,16(3):14. [4] ZHANG Y S,Zhang Z Y,Sugiura N,et al. Biomass & Bioenergy,2002,22:489. [5] YE Hua-jun,LIU Li-peng,XIA A-lin,et al(叶华俊, 刘立鹏,夏阿林, 等). Chinese Journal of Scientific Instrument(仪器仪表学报),2009,30(3):531. [6] Inmaculada G M,Claudio G P,Jesus H M,et al. Analytica Chimica Acta,2002,453(2):281. [7] Blanco M,Serrano D. The Analyst,2000,125(11):2059. [8] Workman J,Jr K M,Veltkamp D. Analytical Chemistry,2007,79(12):4345. [9] Chung H,Ku M S. Vibrational Spectroscopy,2003,31:125. [10] ASTM E1655-05. American Society for Testing Materials(美国材料与试验协会), 2005.