Determination of Inorganic Elements in Elsholtzia bodinieri Vaniot from Gansu by Microwave Digestion ICP-AES
HU Hao-bin1*, CAO Hong2, LIU Jian-xin3, ZHENG Xu-dong1
1. Department of Chemistry, Longdong University, Qingyang 745000, China 2. Department of Agronomy, Longdong University, Qingyang 745000, China 3. Department of Life Science, Longdong University, Qingyang 745000, China
Abstract:In the present paper, orthogonal test and square error analysis were applied to the determination of inorganic elements in the aerial part of E. bodinieri V. such as K, Na, Ca, Ba, Pb, Zn, Mn, Cu, Mg, Fe and Al by microwave digestion ICP-AES technique. The method is simple, rapid, and features of high sensitivity, good accuracy and simultaneous determination of many elements. Its recovery ratio obtained by standard addition method ranged from 93.2% to 104.1%, and its RSD (n=5) was lower than 3.20%. The results showed that this plant has rich inorganic elements, which are essential to human health. The result provides a theoretical basis for investigating the correlation of element content and the effect of medicine in E. bodinieri V.
Key words:Orthogonal test;Square error analysis;ICP-AES;Microwave digestion;Elsholtzia bodinieri Vaniot;Inorganic elements
胡浩斌1, 曹宏2, 刘建新3, 郑旭东1. 微波溶样ICP-AES法测定甘肃东紫苏中的无机元素[J]. 光谱学与光谱分析, 2006, 26(11): 2130-2133.
HU Hao-bin1*, CAO Hong2, LIU Jian-xin3, ZHENG Xu-dong1. Determination of Inorganic Elements in Elsholtzia bodinieri Vaniot from Gansu by Microwave Digestion ICP-AES. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(11): 2130-2133.
[1] Delectis Florae Reipublicae Popularis Sinicae Agendae Academiae Sinicae Edita(中国科学院中国植物志编辑委员会). Flora Reipublicae Popularis Sinicae(中国植物志). Beijing: Science Press(北京: 科学出版社), 1977. 66,336. [2] Jiangsu New Medical College(江苏新医学院). The Big Dictionary of Chinese Traditional and Herbal Drug(中药大辞典). Shanghai: Shanghai Science and Technology Press(上海: 上海科学技术出版社), 1985. 489. [3] ZOU Hai-jian, TANG Zi-ming, WEI Qun-hui, et al(邹海舰, 唐自明, 韦群辉, 等). Journal of Chinese Traditional Folk Medicine(中国民族民间医药杂志), 1999, 41: 359. [4] CHENG Wei-xian, GU Kun, LI Cong, et al(程伟贤, 古 昆, 李 聪, 等). Journal of Yunnan Nationalities University(云南民族大学学报), 2004, 13(2): 86. [5] HU Hao-bin, ZHENG Xu-dong(胡浩斌, 郑旭东). The Chinese Academic Medical Magazine of Organisms(中国医学生物技术应用杂志), 2004, 3(4): 35. [6] HU Hao-bin, JIAN Yu-feng, LIU Jian-xin, et al(胡浩斌, 简毓峰, 刘建新, 等). The Chinese Academic Medical Magazine of Organisms(中国医学生物技术应用杂志), 2005, 4(2): 74. [7] CHENG Yi-yong, JIANG Yu-gang(程义勇, 蒋与刚). The Databook of Biomedical Trace Elements(生物医学微量元素数据手册). Tianjin: Tianjin Science and Technology Press(天津: 天津科学技术出版社), 1994. 8. [8] LIU Yan-ming(刘彦明). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2000, 20(3): 373. [9] LIU Ying, LI Jing-feng, GA Ri-di, et al(刘 颖,李景峰,嘎日迪,等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2006,26(2):344.