Study of Inorganic Elements in Silybum Marianum: Distribution and Extraction Rate
CAI Xiu-lan, CHEN Yi-jun, DAI Le-mei, LIAN Hong-zhen*
Key Laboratory of Analytical Chemistry for Life Science, Ministry of Education, Center of Materials Analysis, Department of Chemistry, Nanjing University, Nanjing 210093, China
Abstract：The contents of multiple inorganic elements in silybum marianum products in different processing stages, including dry fruit, seedcake and extracts, were simultaneously measured by inductively coupled plasma atom emission spectrometry (ICP-AES) and inductively coupled plasma mass spectrometry (ICP-MS). The results indicated that the contents of the elements are the highest in the seedcake and the lowest in the extracts. Moreover, the different decoctions of Silybum marianum fruit made for different immersion times were determined. It was demonstrated that most of the elements measured are soluble, and the total content extracted for the first four immersion times is much higher than that for the latter three times. The certificate reference tea (GBW070605) was analyzed by this method, and the analysis results of most elements in the reference tea were in agreement with the certified values.
Key words：ICP-AES;ICP-MS;Silybum marianum;Inorganic elements
蔡秀兰，陈逸珺，戴乐美，练鸿振*. 水飞蓟中无机元素的含量分布及溶出性质的研究[J]. 光谱学与光谱分析, 2006, 26(11): 2125-2129.
CAI Xiu-lan, CHEN Yi-jun, DAI Le-mei, LIAN Hong-zhen*. Study of Inorganic Elements in Silybum Marianum: Distribution and Extraction Rate. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(11): 2125-2129.
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